The effect of concentration extender on the making of lignin phenol-formaldehyde from coconut fibre as an environmentally friendly adhesive

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Yusmaniar, F. Kurniadewi, A. Nur Oktavia

2023 Journal of Physics: Conference Series Vol. 2498 Issue 1 Conference paper Cited by 0 SDG 12 Quartile

Abstract

This study aims to make adhesives with a variety of concentration extenders. First, the coconut husk was delignified with 25% NaOH and then precipitated with sulfuric acid. The yield of lignin from coconut coir was 38.92%, with a purity of 68%, a phenolic hydroxyl content of 2.47%, and an equivalent molecular weight of 1666.67 g/mol. Lignin was then used to synthesize phenol-formaldehyde (LPF) lignin by adding tapioca flour extender with variations of 10%, 20% and 30% of the mass of phenol through the resol method with 50% NaOH catalyst. Then the characterization was carried out using FTIR Spectrophotometer, XRD and adhesive test. The results showed that the LPF copolymer with a 10% extender was better than the LPF copolymer without an extender for wood adhesives with adhesive resistance of 955.34 N and low formaldehyde emission of 0.44 mg/L. © Published under licence by IOP Publishing Ltd.

Affiliations

Department of Chemistry, State University of Jakarta, Jl. Rawamangun Muka, Jakarta, 13220, Indonesia

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